Amide bond formation of sialic acid in oligosaccharide without protecting group

Shino Manabe, Junpei Abe, Yukishige Ito

Research output: Contribution to journalArticlepeer-review

4 Citations (Scopus)

Abstract

– With the aim of preparing glycan-linked antibody-drug conjugates, we investigated the feasibility of amide bond formation at the carboxylic acid of sialic acid in a protection-free oligosaccharide. The use of a phosphonium salt-based reagent, PyBOP, gave the desired compound. Bio-orthogonal functional groups were conjugated at the carboxylic acid site of sialic acid in glycans.

Original languageEnglish
Pages (from-to)1203-1209
Number of pages7
JournalHeterocycles
Volume97
Issue number2
DOIs
Publication statusPublished - 2018

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