Bracket bond strength and cariostatic potential of an experimental resin adhesive system containing Portland cement

Masahiro Iijima, Masanori Hashimoto, Susumu Nakagaki, Takeshi Muguruma, Naohisa Kohda, Kazuhiko Endo, Itaru Mizoguchi

Research output: Contribution to journalArticlepeer-review

2 Citations (Scopus)


Objective: To determine if a new experimental resin-based material containing Portland cement (PC) can help prevent enamel caries while providing adequate shear bond strength (SBS). Materials and Methods: Brackets were bonded to human premolars with experimental resinbased adhesive pastes composed of three weight rations of resin and PC powder (PC 30, 7:3; PC 50, 5:5; PC 70, 3:7; n 5 7). Self-etching primer (SEP) adhesive (Transbond Plus) and resinmodified glass ionomer cement (RMGIC) adhesive (Fuji Ortho FC Automix) were used for comparison. All of the bonded teeth were subjected to alternating immersion in demineralizing (pH 4.55) and remineralizing (pH 6.8) solutions for 14 days. The SBS for each sample was examined, and the Adhesive Remnant Index (ARI) score was calculated. The hardness and elastic modulus of the enamel were determined by a nanoindenter at 20 equidistant depths from the external surface at 100 mm from the bracket edge. Data were compared by one-way analysis of variance and a chi-square test. Results: PC 50 and PC 70 showed significantly greater SBS than Fuji Ortho FC Automix, although Transbond Plus showed significantly greater SBS than other bonding systems. No significant difference in the ARI category was observed among the five groups. For specimens bonded with PC 50 and PC 70, the hardness and elastic modulus values in most locations were equivalent to those of Fuji Ortho FC Automix. Conclusions: Experimental resin-based bonding material containing PC provides adequate SBS and a caries-preventive effect equivalent to that of the RMGIC adhesive system.

Original languageEnglish
Pages (from-to)900-906
Number of pages7
JournalAngle Orthodontist
Issue number5
Publication statusPublished - 2012 Sept


  • Adhesive
  • Demineralization
  • Nanoindentation
  • Portland cement
  • Shear bond strength


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