Consolidation of nano-sized TiN powders by spark plasma sintering

Lianjun Wang; Wan Jiang; Lidong Chen; Mei Yang; Hongmin Zhu

doi:10.1111/j.1551-2916.2006.01066.x

Consolidation of nano-sized TiN powders by spark plasma sintering

Lianjun Wang, Wan Jiang, Lidong Chen, Mei Yang, Hongmin Zhu

ENG - Metallurgy

Research output: Contribution to journal › Article › peer-review

46 Citations (Scopus)

Abstract

Nano-sized TiN powders with an average particle size of 19 nm were synthesized via a new method, reduction-nitridation reaction in liquid ammonia. A consolidation procedure using spark plasma sintering (SPS) was used, and a dense TiN ceramic (> 98% of theoretical) with mean grain size of 100-150 nm was obtained at 1380°C. The influence of sintering temperature on grain growth and microstructural evolution was also discussed.

Original language	English
Pages (from-to)	2364-2366
Number of pages	3
Journal	Journal of the American Ceramic Society
Volume	89
Issue number	7
DOIs	https://doi.org/10.1111/j.1551-2916.2006.01066.x
Publication status	Published - 2006 Jul

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10.1111/j.1551-2916.2006.01066.x

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abstract = "Nano-sized TiN powders with an average particle size of 19 nm were synthesized via a new method, reduction-nitridation reaction in liquid ammonia. A consolidation procedure using spark plasma sintering (SPS) was used, and a dense TiN ceramic (> 98% of theoretical) with mean grain size of 100-150 nm was obtained at 1380°C. The influence of sintering temperature on grain growth and microstructural evolution was also discussed.",

author = "Lianjun Wang and Wan Jiang and Lidong Chen and Mei Yang and Hongmin Zhu",

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AU - Wang, Lianjun

AU - Jiang, Wan

AU - Chen, Lidong

AU - Yang, Mei

AU - Zhu, Hongmin

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AB - Nano-sized TiN powders with an average particle size of 19 nm were synthesized via a new method, reduction-nitridation reaction in liquid ammonia. A consolidation procedure using spark plasma sintering (SPS) was used, and a dense TiN ceramic (> 98% of theoretical) with mean grain size of 100-150 nm was obtained at 1380°C. The influence of sintering temperature on grain growth and microstructural evolution was also discussed.

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ER -

Consolidation of nano-sized TiN powders by spark plasma sintering

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