TY - JOUR
T1 - Crystallization behavior of optical fibers with multi layered structure for nonlinear optical devices
AU - Iwafuchi, Naoki
AU - Masai, Hirokazu
AU - Takahashi, Yoshihiro
AU - Fujiwara, Takumi
AU - Ohara, Seiki
AU - Kondo, Yuki
AU - Sugimoto, Naoki
PY - 2008/10
Y1 - 2008/10
N2 - We examined the crystallization behavior of double clad fiber composed by BaO-TiO2-GeO2-SiO2 based glasses in detail. Formation of needle-like fresnoite-type Ba2Ti(Ge,Si) 2O8 were observed at the interface between the first and second clad. In addition, we employed the two-step heat-treatment (i.e., 728°C, 20 h + 749°C, 1 h) in fabrication of the crystallized fiber in order to obtain the highly-oriented fresnoite phase in the fiber structure. The first treating temperature, 728°C, which gives the maximum nucleation rate, was determined by differential thermal analysis. It was demonstrated that the two-step heat-treatment was effective for improvement of the orientation of fresnoite-type phase in the first clad of the double clad fiber.
AB - We examined the crystallization behavior of double clad fiber composed by BaO-TiO2-GeO2-SiO2 based glasses in detail. Formation of needle-like fresnoite-type Ba2Ti(Ge,Si) 2O8 were observed at the interface between the first and second clad. In addition, we employed the two-step heat-treatment (i.e., 728°C, 20 h + 749°C, 1 h) in fabrication of the crystallized fiber in order to obtain the highly-oriented fresnoite phase in the fiber structure. The first treating temperature, 728°C, which gives the maximum nucleation rate, was determined by differential thermal analysis. It was demonstrated that the two-step heat-treatment was effective for improvement of the orientation of fresnoite-type phase in the first clad of the double clad fiber.
KW - Glass ceramics
KW - Nonlinear optics
KW - Optical device
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U2 - 10.2109/jcersj2.116.1115
DO - 10.2109/jcersj2.116.1115
M3 - Article
AN - SCOPUS:54249124616
SN - 1882-0743
VL - 116
SP - 1115
EP - 1120
JO - Journal of the Ceramic Society of Japan
JF - Journal of the Ceramic Society of Japan
IS - 1358
ER -