Influence of Fe addition to hydroxyapatite by hydrothermal process

Mitsutaka Sato, Atsushi Nakahira

Research output: Contribution to journalArticlepeer-review

7 Citations (Scopus)

Abstract

In order to develop non toxic magnetic beads, influence of Fe addition to the hydroxyapatite was investigated, and Fe doped hydroxyapatite was prepared by hydrothermal process at 423K. The crystal phase of obtained samples had a hydroxyapatite related structure, and α-Fe2O3phase generated as a second phase at the ratio of Fe more than 5mol% additions. The ratio of α-Fe2O3 phase increased depending on the ratio of Fe, and 40 and 73% of added Fe existed as α-Fe2O 3 phase at 5 and 10mol % addition, and the estimated doped amount of Fe is about 2.1 mol% for 5mol% addition and 2.7 mol% for 10mol% addition, respectively. All samples showed paramagnetic property, and magnetization of sample increased depending on the ratio of Fe. The maximum magnetization of 0.63 Am2/kg was obtained at the Fe ratio of 10 mol %.

Original languageEnglish
Pages (from-to)559-562
Number of pages4
JournalJournal of the Ceramic Society of Japan
Volume121
Issue number1415
DOIs
Publication statusPublished - 2013 Jul

Keywords

  • Drug delivery system
  • Hydrothermal process
  • Magnetic property
  • XAFS

ASJC Scopus subject areas

  • Ceramics and Composites
  • Chemistry(all)
  • Condensed Matter Physics
  • Materials Chemistry

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