Mechanical behavior law of ceramic nanoparticles from transmission electron microscopy in situ nano-compression tests

E. Calvié; J. Réthoré; L. Joly-Pottuz; S. Meille; J. Chevalier; V. Garnier; Y. Jorand; C. Esnouf; T. Epicier; J. B. Quirk; K. Masenelli-Varlot

doi:10.1016/j.matlet.2014.01.002

Mechanical behavior law of ceramic nanoparticles from transmission electron microscopy in situ nano-compression tests

E. Calvié, J. Réthoré, L. Joly-Pottuz, S. Meille, J. Chevalier, V. Garnier, Y. Jorand, C. Esnouf, T. Epicier, J. B. Quirk, K. Masenelli-Varlot

Research output: Contribution to journal › Article › peer-review

26 Citations (Scopus)

Abstract

A methodology has been developed to determine constitutive laws of nanoparticles from in situ nano-compression experiments in a transmission electron microscope. It is based on image analysis to obtain relevant load-displacement curves, followed by finite element analysis associated to an inverse method. A transition alumina, stable only at the nanometer size, has been characterized as an example. The Young modulus and yield strength of this transition alumina, not available for such crystallographic structure, have been obtained.

Original language	English
Pages (from-to)	107-110
Number of pages	4
Journal	Materials Letters
Volume	119
DOIs	https://doi.org/10.1016/j.matlet.2014.01.002
Publication status	Published - 2014 Mar 15
Externally published	Yes

Keywords

Ceramics
In situ testing
Nanoparticles
Transmission electron microscopy

ASJC Scopus subject areas

Materials Science(all)
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

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10.1016/j.matlet.2014.01.002

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title = "Mechanical behavior law of ceramic nanoparticles from transmission electron microscopy in situ nano-compression tests",

abstract = "A methodology has been developed to determine constitutive laws of nanoparticles from in situ nano-compression experiments in a transmission electron microscope. It is based on image analysis to obtain relevant load-displacement curves, followed by finite element analysis associated to an inverse method. A transition alumina, stable only at the nanometer size, has been characterized as an example. The Young modulus and yield strength of this transition alumina, not available for such crystallographic structure, have been obtained.",

keywords = "Ceramics, In situ testing, Nanoparticles, Transmission electron microscopy",

author = "E. Calvi{\'e} and J. R{\'e}thor{\'e} and L. Joly-Pottuz and S. Meille and J. Chevalier and V. Garnier and Y. Jorand and C. Esnouf and T. Epicier and Quirk, {J. B.} and K. Masenelli-Varlot",

note = "Funding Information: Acknowledgments to the Centre Lyonnais de Microscopie (CLYM; http://www.clym.fr) for the access to the JEOL 2010F, to Region Rhone-Alpes (Cluster MACODEV) and the Institut Universitaire de France for financial support, and Stephane Pailhes, ILM University Lyon, for the high pressure experiments.",

year = "2014",

month = mar,

day = "15",

doi = "10.1016/j.matlet.2014.01.002",

language = "English",

volume = "119",

pages = "107--110",

journal = "Materials Letters",

issn = "0167-577X",

publisher = "Elsevier",

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TY - JOUR

T1 - Mechanical behavior law of ceramic nanoparticles from transmission electron microscopy in situ nano-compression tests

AU - Calvié, E.

AU - Réthoré, J.

AU - Joly-Pottuz, L.

AU - Meille, S.

AU - Chevalier, J.

AU - Garnier, V.

AU - Jorand, Y.

AU - Esnouf, C.

AU - Epicier, T.

AU - Quirk, J. B.

AU - Masenelli-Varlot, K.

N1 - Funding Information: Acknowledgments to the Centre Lyonnais de Microscopie (CLYM; http://www.clym.fr) for the access to the JEOL 2010F, to Region Rhone-Alpes (Cluster MACODEV) and the Institut Universitaire de France for financial support, and Stephane Pailhes, ILM University Lyon, for the high pressure experiments.

PY - 2014/3/15

Y1 - 2014/3/15

N2 - A methodology has been developed to determine constitutive laws of nanoparticles from in situ nano-compression experiments in a transmission electron microscope. It is based on image analysis to obtain relevant load-displacement curves, followed by finite element analysis associated to an inverse method. A transition alumina, stable only at the nanometer size, has been characterized as an example. The Young modulus and yield strength of this transition alumina, not available for such crystallographic structure, have been obtained.

AB - A methodology has been developed to determine constitutive laws of nanoparticles from in situ nano-compression experiments in a transmission electron microscope. It is based on image analysis to obtain relevant load-displacement curves, followed by finite element analysis associated to an inverse method. A transition alumina, stable only at the nanometer size, has been characterized as an example. The Young modulus and yield strength of this transition alumina, not available for such crystallographic structure, have been obtained.

KW - Ceramics

KW - In situ testing

KW - Nanoparticles

KW - Transmission electron microscopy

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DO - 10.1016/j.matlet.2014.01.002

M3 - Article

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VL - 119

SP - 107

EP - 110

JO - Materials Letters

JF - Materials Letters

ER -

Mechanical behavior law of ceramic nanoparticles from transmission electron microscopy in situ nano-compression tests

Abstract

Keywords

ASJC Scopus subject areas

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