One-pot reductive cleavage of exo-olefin to methylene with a mild ozonolysis-Clemmensen reduction sequence

Shu Xu, Takayuki Toyama, Jun Nakamura, Hirokazu Arimoto

Research output: Contribution to journalArticlepeer-review

29 Citations (Scopus)

Abstract

A one-pot exo-olefin reductive cleavage was for the first time developed. The reaction could proceed under a mild condition avoiding the use of hazardous and expensive reagents. Meanwhile, a TMSCl-mediated Clemmensen reduction in alcoholic solvent was also examined.

Original languageEnglish
Pages (from-to)4534-4537
Number of pages4
JournalTetrahedron Letters
Volume51
Issue number34
DOIs
Publication statusPublished - 2010 Aug 25

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