TY - JOUR
T1 - Rapid preparation of YBa2Cu3O7-x with Tc ∼ 90 K using a domestic microwave oven
AU - Kato, Masatsune
AU - Sakakibara, Kenji
AU - Koike, Yoji
PY - 1997/10/1
Y1 - 1997/10/1
N2 - High-Tc superconducting samples of YBa2Cu3O7-cursive Greek chi with Tc ∼ 90 K have been prepared in a short time of 25 min, using a domestic microwave oven operated at 2.45 GHz and 200 W, without any post-heat treatment. Post-heat treatment is not necessary due to improvement of the sample environment during the microwave process. That is, a pellet of mixed powders of raw materials is surrounded by mixed powders of raw matetials and subsequenty wrapped in glass wool, in order to suppress rapid dissipation of heat from the surface of the pellet. This leads to successful preparation of homogeneous and oxygenated samples of YBa2Cu3O7-cursive Greek chi.
AB - High-Tc superconducting samples of YBa2Cu3O7-cursive Greek chi with Tc ∼ 90 K have been prepared in a short time of 25 min, using a domestic microwave oven operated at 2.45 GHz and 200 W, without any post-heat treatment. Post-heat treatment is not necessary due to improvement of the sample environment during the microwave process. That is, a pellet of mixed powders of raw materials is surrounded by mixed powders of raw matetials and subsequenty wrapped in glass wool, in order to suppress rapid dissipation of heat from the surface of the pellet. This leads to successful preparation of homogeneous and oxygenated samples of YBa2Cu3O7-cursive Greek chi.
KW - Domestic microwave oven
KW - Electrical resistivity
KW - High-T superconductor
KW - Magnetic susceptibility
KW - Sample preparation
KW - YBaCuO
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UR - http://www.scopus.com/inward/citedby.url?scp=0031246079&partnerID=8YFLogxK
U2 - 10.1143/jjap.36.l1291
DO - 10.1143/jjap.36.l1291
M3 - Article
AN - SCOPUS:0031246079
SN - 0021-4922
VL - 36
SP - L1291-L1293
JO - Japanese Journal of Applied Physics
JF - Japanese Journal of Applied Physics
IS - 10 PART A
ER -