Selective synthesis of the C3v isomer of C60H 18

Thomas Wågberg; Dan Johnels; Ashgar Peera; Mattias Hedenström; Yury M. Schulga; Yury O. Tsybin; J. M. Purcell; Alan G. Marshall; Dag Noreus; Toyoto Sato; Alexandr V. Talyzin

doi:10.1021/ol052175p

Selective synthesis of the C_3v isomer of C₆₀H ₁₈

Thomas Wågberg, Dan Johnels, Ashgar Peera, Mattias Hedenström, Yury M. Schulga, Yury O. Tsybin, J. M. Purcell, Alan G. Marshall, Dag Noreus, Toyoto Sato, Alexandr V. Talyzin

Research output: Contribution to journal › Article › peer-review

21 Citations (Scopus)

Abstract

(Figure Presented) C₆₀H₁₈ has been produced by hydrogenation of C₆₀ at 100 bar H₂ pressure and 673 K for 10 h. We have investigated the crude material without any purification by use of ¹H NMR, ¹³C NMR, and IR spectroscopy and Fourier transform ion cyclotron resonance mass spectrometry. We show that the crude material consists of 95% of the C_3v isomer of C₆₀H ₁₈.

Original language	English
Pages (from-to)	5557-5560
Number of pages	4
Journal	Organic letters
Volume	7
Issue number	25
DOIs	https://doi.org/10.1021/ol052175p
Publication status	Published - 2005 Dec 8
Externally published	Yes

ASJC Scopus subject areas

Biochemistry
Physical and Theoretical Chemistry
Organic Chemistry

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title = "Selective synthesis of the C3v isomer of C60H 18",

abstract = "(Figure Presented) C60H18 has been produced by hydrogenation of C60 at 100 bar H2 pressure and 673 K for 10 h. We have investigated the crude material without any purification by use of 1H NMR, 13C NMR, and IR spectroscopy and Fourier transform ion cyclotron resonance mass spectrometry. We show that the crude material consists of 95% of the C3v isomer of C60H 18.",

author = "Thomas W{\aa}gberg and Dan Johnels and Ashgar Peera and Mattias Hedenstr{\"o}m and Schulga, {Yury M.} and Tsybin, {Yury O.} and Purcell, {J. M.} and Marshall, {Alan G.} and Dag Noreus and Toyoto Sato and Talyzin, {Alexandr V.}",

year = "2005",

month = dec,

day = "8",

doi = "10.1021/ol052175p",

language = "English",

volume = "7",

pages = "5557--5560",

journal = "Organic Letters",

issn = "1523-7060",

publisher = "American Chemical Society",

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TY - JOUR

T1 - Selective synthesis of the C3v isomer of C60H 18

AU - Wågberg, Thomas

AU - Johnels, Dan

AU - Peera, Ashgar

AU - Hedenström, Mattias

AU - Schulga, Yury M.

AU - Tsybin, Yury O.

AU - Purcell, J. M.

AU - Marshall, Alan G.

AU - Noreus, Dag

AU - Sato, Toyoto

AU - Talyzin, Alexandr V.

PY - 2005/12/8

Y1 - 2005/12/8

N2 - (Figure Presented) C60H18 has been produced by hydrogenation of C60 at 100 bar H2 pressure and 673 K for 10 h. We have investigated the crude material without any purification by use of 1H NMR, 13C NMR, and IR spectroscopy and Fourier transform ion cyclotron resonance mass spectrometry. We show that the crude material consists of 95% of the C3v isomer of C60H 18.

AB - (Figure Presented) C60H18 has been produced by hydrogenation of C60 at 100 bar H2 pressure and 673 K for 10 h. We have investigated the crude material without any purification by use of 1H NMR, 13C NMR, and IR spectroscopy and Fourier transform ion cyclotron resonance mass spectrometry. We show that the crude material consists of 95% of the C3v isomer of C60H 18.

UR - http://www.scopus.com/inward/record.url?scp=29444458960&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=29444458960&partnerID=8YFLogxK

U2 - 10.1021/ol052175p

DO - 10.1021/ol052175p

M3 - Article

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AN - SCOPUS:29444458960

SN - 1523-7060

VL - 7

SP - 5557

EP - 5560

JO - Organic Letters

JF - Organic Letters

IS - 25

ER -

Selective synthesis of the C_3v isomer of C₆₀H ₁₈

Abstract

ASJC Scopus subject areas

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