Simultaneous determination of the composition and size of oxide particles in solid materials by laser ablation-inductively coupled plasma mass spectrometry

Andrey V. Karasev; Ryo Inoue

doi:10.2320/matertrans.MRA2008301

Simultaneous determination of the composition and size of oxide particles in solid materials by laser ablation-inductively coupled plasma mass spectrometry

Andrey V. Karasev, Ryo Inoue

Institute of Multidisciplinary Research for Advanced Materials (IMRAM)

Research output: Contribution to journal › Article › peer-review

5 Citations (Scopus)

Abstract

Laser ablation-inductively coupled plasma mass spectrometry (LA-ICP-MS) has been used for the determination of the composition and size of oxide particles consisting of SiO₂, MnO, Al₂O₃, MgO and CaO on the surface of a glass or metal sample. The composition and size of multicomponent oxide particles such as MnO-SiO₂, CaO-Al ₂O₃ and CaO-Al₂O₃-MgO evaluated by LA-ICP-MS are compared with those obtained by chemical analysis and by SEM observation. It is confirmed that LA-ICP-MS method has prospects to be applied for quick and simultaneous measurement of the composition and size of particles on the surface of metals in steelmaking industry. The difference between the particle size determined by LA-ICP-MS and that by SEM ranges from 6 to 13% on an average in the range of d_V = 7-40 μm.

Original language	English
Pages (from-to)	341-348
Number of pages	8
Journal	Materials Transactions
Volume	50
Issue number	2
DOIs	https://doi.org/10.2320/matertrans.MRA2008301
Publication status	Published - 2009 Feb

Keywords

Inclusion
Inductively coupled plasma
Laser ablation
Mass spectrometry
Oxide particle

ASJC Scopus subject areas

Materials Science(all)
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

Access to Document

10.2320/matertrans.MRA2008301

Cite this

@article{f942b11578cb462b864c33d9447ffbbe,

title = "Simultaneous determination of the composition and size of oxide particles in solid materials by laser ablation-inductively coupled plasma mass spectrometry",

abstract = "Laser ablation-inductively coupled plasma mass spectrometry (LA-ICP-MS) has been used for the determination of the composition and size of oxide particles consisting of SiO2, MnO, Al2O3, MgO and CaO on the surface of a glass or metal sample. The composition and size of multicomponent oxide particles such as MnO-SiO2, CaO-Al 2O3 and CaO-Al2O3-MgO evaluated by LA-ICP-MS are compared with those obtained by chemical analysis and by SEM observation. It is confirmed that LA-ICP-MS method has prospects to be applied for quick and simultaneous measurement of the composition and size of particles on the surface of metals in steelmaking industry. The difference between the particle size determined by LA-ICP-MS and that by SEM ranges from 6 to 13% on an average in the range of dV = 7-40 μm.",

keywords = "Inclusion, Inductively coupled plasma, Laser ablation, Mass spectrometry, Oxide particle",

author = "Karasev, {Andrey V.} and Ryo Inoue",

year = "2009",

month = feb,

doi = "10.2320/matertrans.MRA2008301",

language = "English",

volume = "50",

pages = "341--348",

journal = "Materials Transactions",

issn = "1345-9678",

publisher = "Japan Institute of Metals (JIM)",

number = "2",

}

TY - JOUR

T1 - Simultaneous determination of the composition and size of oxide particles in solid materials by laser ablation-inductively coupled plasma mass spectrometry

AU - Karasev, Andrey V.

AU - Inoue, Ryo

PY - 2009/2

Y1 - 2009/2

N2 - Laser ablation-inductively coupled plasma mass spectrometry (LA-ICP-MS) has been used for the determination of the composition and size of oxide particles consisting of SiO2, MnO, Al2O3, MgO and CaO on the surface of a glass or metal sample. The composition and size of multicomponent oxide particles such as MnO-SiO2, CaO-Al 2O3 and CaO-Al2O3-MgO evaluated by LA-ICP-MS are compared with those obtained by chemical analysis and by SEM observation. It is confirmed that LA-ICP-MS method has prospects to be applied for quick and simultaneous measurement of the composition and size of particles on the surface of metals in steelmaking industry. The difference between the particle size determined by LA-ICP-MS and that by SEM ranges from 6 to 13% on an average in the range of dV = 7-40 μm.

AB - Laser ablation-inductively coupled plasma mass spectrometry (LA-ICP-MS) has been used for the determination of the composition and size of oxide particles consisting of SiO2, MnO, Al2O3, MgO and CaO on the surface of a glass or metal sample. The composition and size of multicomponent oxide particles such as MnO-SiO2, CaO-Al 2O3 and CaO-Al2O3-MgO evaluated by LA-ICP-MS are compared with those obtained by chemical analysis and by SEM observation. It is confirmed that LA-ICP-MS method has prospects to be applied for quick and simultaneous measurement of the composition and size of particles on the surface of metals in steelmaking industry. The difference between the particle size determined by LA-ICP-MS and that by SEM ranges from 6 to 13% on an average in the range of dV = 7-40 μm.

KW - Inclusion

KW - Inductively coupled plasma

KW - Laser ablation

KW - Mass spectrometry

KW - Oxide particle

UR - http://www.scopus.com/inward/record.url?scp=63149169587&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=63149169587&partnerID=8YFLogxK

U2 - 10.2320/matertrans.MRA2008301

DO - 10.2320/matertrans.MRA2008301

M3 - Article

AN - SCOPUS:63149169587

SN - 1345-9678

VL - 50

SP - 341

EP - 348

JO - Materials Transactions

JF - Materials Transactions

IS - 2

ER -

Simultaneous determination of the composition and size of oxide particles in solid materials by laser ablation-inductively coupled plasma mass spectrometry

Abstract

Keywords

ASJC Scopus subject areas

Access to Document

Other files and links

Fingerprint

Cite this