Single crystal growth of wadsleyite

Anton Shatskiy; Konstantin D. Litasasov; Takuya Matsuzaki; Keiji Shinodada; Daisuke Yamaamaamazaki; Akira Yonedada; Eiji Ito; Tomoo Katsura

doi:10.2138/am.2009.3150

Single crystal growth of wadsleyite

Anton Shatskiy, Konstantin D. Litasasov, Takuya Matsuzaki, Keiji Shinodada, Daisuke Yamaamaamazaki, Akira Yonedada, Eiji Ito, Tomoo Katsura

Research output: Contribution to journal › Article › peer-review

15 Citations (Scopus)

Abstract

We have synthesized large (0.7-1.0 mm) crystals of anhydrous, water-bearing, and Fe-bearing wadsleyite by means of growth from solution in the thermal gradient field. Nearly anhydrous (<68±4 wt ppm H ₂O) Mg₂SiO₄ crystals were grown using K ₂Mg(CO₃)₂ as a solvent at 16.5 GPa and 1700 °C. (Mg_0.92Fe_0.08)₂SiO₄ crystals containing 84±17 wt ppm H₂O were grown using 92K ₂Mg(CO₃)₂-8FeCl₂ as a solvent. Crystals of Fe-free wadsleyite with 1496±117 wt ppm H2O were synthesized at 1400 °C and 15.5 GPa by using 2KHCO₃-Mg(OH)₂ as a solvent.

Original language	English
Pages (from-to)	1130-1136
Number of pages	7
Journal	American Mineralogist
Volume	94
Issue number	8-9
DOIs	https://doi.org/10.2138/am.2009.3150
Publication status	Published - 2009
Externally published	Yes

Keywords

High pressure
Single crystal growth
Thermal gradient method
Wadsleyite

ASJC Scopus subject areas

Geophysics
Geochemistry and Petrology

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10.2138/am.2009.3150

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title = "Single crystal growth of wadsleyite",

abstract = "We have synthesized large (0.7-1.0 mm) crystals of anhydrous, water-bearing, and Fe-bearing wadsleyite by means of growth from solution in the thermal gradient field. Nearly anhydrous (<68±4 wt ppm H 2O) Mg2SiO4 crystals were grown using K 2Mg(CO3)2 as a solvent at 16.5 GPa and 1700 °C. (Mg0.92Fe0.08)2SiO4 crystals containing 84±17 wt ppm H2O were grown using 92K 2Mg(CO3)2-8FeCl2 as a solvent. Crystals of Fe-free wadsleyite with 1496±117 wt ppm H2O were synthesized at 1400 °C and 15.5 GPa by using 2KHCO3-Mg(OH)2 as a solvent.",

keywords = "High pressure, Single crystal growth, Thermal gradient method, Wadsleyite",

author = "Anton Shatskiy and Litasasov, {Konstantin D.} and Takuya Matsuzaki and Keiji Shinodada and Daisuke Yamaamaamazaki and Akira Yonedada and Eiji Ito and Tomoo Katsura",

year = "2009",

doi = "10.2138/am.2009.3150",

language = "English",

volume = "94",

pages = "1130--1136",

journal = "American Mineralogist",

issn = "0003-004X",

publisher = "Mineralogical Society of America",

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TY - JOUR

T1 - Single crystal growth of wadsleyite

AU - Shatskiy, Anton

AU - Litasasov, Konstantin D.

AU - Matsuzaki, Takuya

AU - Shinodada, Keiji

AU - Yamaamaamazaki, Daisuke

AU - Yonedada, Akira

AU - Ito, Eiji

AU - Katsura, Tomoo

PY - 2009

Y1 - 2009

N2 - We have synthesized large (0.7-1.0 mm) crystals of anhydrous, water-bearing, and Fe-bearing wadsleyite by means of growth from solution in the thermal gradient field. Nearly anhydrous (<68±4 wt ppm H 2O) Mg2SiO4 crystals were grown using K 2Mg(CO3)2 as a solvent at 16.5 GPa and 1700 °C. (Mg0.92Fe0.08)2SiO4 crystals containing 84±17 wt ppm H2O were grown using 92K 2Mg(CO3)2-8FeCl2 as a solvent. Crystals of Fe-free wadsleyite with 1496±117 wt ppm H2O were synthesized at 1400 °C and 15.5 GPa by using 2KHCO3-Mg(OH)2 as a solvent.

AB - We have synthesized large (0.7-1.0 mm) crystals of anhydrous, water-bearing, and Fe-bearing wadsleyite by means of growth from solution in the thermal gradient field. Nearly anhydrous (<68±4 wt ppm H 2O) Mg2SiO4 crystals were grown using K 2Mg(CO3)2 as a solvent at 16.5 GPa and 1700 °C. (Mg0.92Fe0.08)2SiO4 crystals containing 84±17 wt ppm H2O were grown using 92K 2Mg(CO3)2-8FeCl2 as a solvent. Crystals of Fe-free wadsleyite with 1496±117 wt ppm H2O were synthesized at 1400 °C and 15.5 GPa by using 2KHCO3-Mg(OH)2 as a solvent.

KW - High pressure

KW - Single crystal growth

KW - Thermal gradient method

KW - Wadsleyite

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U2 - 10.2138/am.2009.3150

DO - 10.2138/am.2009.3150

M3 - Article

AN - SCOPUS:76649109253

SN - 0003-004X

VL - 94

SP - 1130

EP - 1136

JO - American Mineralogist

JF - American Mineralogist

IS - 8-9

ER -

Single crystal growth of wadsleyite

Abstract

Keywords

ASJC Scopus subject areas

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