TY - JOUR
T1 - Synthesis of a new birnessite-type compound in K-Mg-Sn-O system
AU - Uheda, K.
AU - Sakuma, J.
AU - Takeuchi, Y.
AU - Takizawa, H.
AU - Endo, T.
AU - Horiuchi, A.
AU - Shimada, M.
N1 - Funding Information:
We would like to thank Mr Michael Crawford for his comments, which improved this letter enormously. This work was supported in part by a Grant-in-Aid for Scientific Research (B) (No.10450237) from the Ministry of Education, Science and Culture, Japan.
PY - 1999/3/1
Y1 - 1999/3/1
N2 - A new birnessite-type compound was prepared in K-Mg-Sn-O system by a solid-state reaction. The resulting phase was characterized by X-ray diffraction (XRD), differential thermal analysis and thermogravimetric analysis (DTA-TGA) and scanning electron microscopic (SEM) analysis. DTA-TGA curves were measured in air to 1200°C at a ramp rate of 10°C min-1. Endothermic peaks at 118°C and 154°C each showed a weight loss. An exothermic peak with a large weight loss associated with potassium was observed at 905°C. SEM revealed the crystal shape and size of the developed phase.
AB - A new birnessite-type compound was prepared in K-Mg-Sn-O system by a solid-state reaction. The resulting phase was characterized by X-ray diffraction (XRD), differential thermal analysis and thermogravimetric analysis (DTA-TGA) and scanning electron microscopic (SEM) analysis. DTA-TGA curves were measured in air to 1200°C at a ramp rate of 10°C min-1. Endothermic peaks at 118°C and 154°C each showed a weight loss. An exothermic peak with a large weight loss associated with potassium was observed at 905°C. SEM revealed the crystal shape and size of the developed phase.
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U2 - 10.1023/A:1006676516299
DO - 10.1023/A:1006676516299
M3 - Article
AN - SCOPUS:0033101295
SN - 0261-8028
VL - 18
SP - 377
EP - 379
JO - Journal of Materials Science Letters
JF - Journal of Materials Science Letters
IS - 5
ER -