Synthesis of bruceantin precursor: 15-deoxybruceolide

Makoto Sasaki; Tatsushi Murae; Takeyoshi Takahashi

doi:10.1016/S0040-4039(00)82238-8

Synthesis of bruceantin precursor: 15-deoxybruceolide

Makoto Sasaki, Tatsushi Murae, Takeyoshi Takahashi

LIF - Molecular and Chemical Life Science

The University of Tokyo

Research output: Contribution to journal › Article › peer-review

5 Citations (Scopus)

Abstract

A 15-deoxybruceolide, 11,12-di-O-acetyl-3-O-t-butyldimethylsilyl ether (3), was synthesized stereoselectively starting from the previously reported ABCE tetracyclic alcohol (5). The authentic sample of 3 was derived from naturally occurring brusatol (2).

Original language	English
Pages (from-to)	5953-5956
Number of pages	4
Journal	Tetrahedron Letters
Volume	29
Issue number	46
DOIs	https://doi.org/10.1016/S0040-4039(00)82238-8
Publication status	Published - 1988

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10.1016/S0040-4039(00)82238-8

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title = "Synthesis of bruceantin precursor: 15-deoxybruceolide",

abstract = "A 15-deoxybruceolide, 11,12-di-O-acetyl-3-O-t-butyldimethylsilyl ether (3), was synthesized stereoselectively starting from the previously reported ABCE tetracyclic alcohol (5). The authentic sample of 3 was derived from naturally occurring brusatol (2).",

author = "Makoto Sasaki and Tatsushi Murae and Takeyoshi Takahashi",

year = "1988",

doi = "10.1016/S0040-4039(00)82238-8",

language = "English",

volume = "29",

pages = "5953--5956",

journal = "Tetrahedron Letters",

issn = "0040-4039",

publisher = "Elsevier Ltd.",

number = "46",

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TY - JOUR

T1 - Synthesis of bruceantin precursor

T2 - 15-deoxybruceolide

AU - Sasaki, Makoto

AU - Murae, Tatsushi

AU - Takahashi, Takeyoshi

PY - 1988

Y1 - 1988

N2 - A 15-deoxybruceolide, 11,12-di-O-acetyl-3-O-t-butyldimethylsilyl ether (3), was synthesized stereoselectively starting from the previously reported ABCE tetracyclic alcohol (5). The authentic sample of 3 was derived from naturally occurring brusatol (2).

AB - A 15-deoxybruceolide, 11,12-di-O-acetyl-3-O-t-butyldimethylsilyl ether (3), was synthesized stereoselectively starting from the previously reported ABCE tetracyclic alcohol (5). The authentic sample of 3 was derived from naturally occurring brusatol (2).

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U2 - 10.1016/S0040-4039(00)82238-8

DO - 10.1016/S0040-4039(00)82238-8

M3 - Article

AN - SCOPUS:0023816470

SN - 0040-4039

VL - 29

SP - 5953

EP - 5956

JO - Tetrahedron Letters

JF - Tetrahedron Letters

IS - 46

ER -

Synthesis of bruceantin precursor: 15-deoxybruceolide

Abstract

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