Synthesis of Li 1+x V 3O 8 by chemical route and its characterization

Selvasekarapandian Subramanian; Sakunthala Ayyasamy; P. Christopher Selvin; M. V. Reddy; B. V.R. Chowdari; Nithya Heller; Arunkumar Dorai; Hema Muthusamy

doi:10.1166/jnn.2012.5362

Synthesis of Li _1+x V ₃O ₈ by chemical route and its characterization

Selvasekarapandian Subramanian, Sakunthala Ayyasamy, P. Christopher Selvin, M. V. Reddy, B. V.R. Chowdari, Nithya Heller, Arunkumar Dorai, Hema Muthusamy

IMRAM - Center for Mineral Processing and Metallurgy (CMPM)

Research output: Contribution to journal › Article › peer-review

2 Citations (Scopus)

Abstract

Lithium trivanadate (Li _1+xV ₃O ₈) nanorods have been synthesized by the simple polymer precursor route using the polymer, polyvinyl pyrrolidone (PVP) as the complexing agent. Thermal behavior of the precursor has been studied by the differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and differential thermal analysis (DTA) techniques. X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) studies confirm the formation of the compound. High resolution scanning electron microscopy (HRSEM) analysis reveals the synthesized Li _1.2V ₃O ₈ particles to be nanorods with an average diameter of 50 nm.

Original language	English
Pages (from-to)	737-742
Number of pages	6
Journal	Journal of Nanoscience and Nanotechnology
Volume	12
Issue number	1
DOIs	https://doi.org/10.1166/jnn.2012.5362
Publication status	Published - 2012

Keywords

Cathode material
Conductivity
Li V O
Nanorods
PVP

Access to Document

10.1166/jnn.2012.5362

Cite this

@article{29af311aa86e4673ad553745c4660db5,

title = "Synthesis of Li 1+x V 3O 8 by chemical route and its characterization",

abstract = "Lithium trivanadate (Li 1+xV 3O 8) nanorods have been synthesized by the simple polymer precursor route using the polymer, polyvinyl pyrrolidone (PVP) as the complexing agent. Thermal behavior of the precursor has been studied by the differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and differential thermal analysis (DTA) techniques. X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) studies confirm the formation of the compound. High resolution scanning electron microscopy (HRSEM) analysis reveals the synthesized Li 1.2V 3O 8 particles to be nanorods with an average diameter of 50 nm.",

keywords = "Cathode material, Conductivity, Li V O, Nanorods, PVP",

author = "Selvasekarapandian Subramanian and Sakunthala Ayyasamy and Selvin, {P. Christopher} and Reddy, {M. V.} and Chowdari, {B. V.R.} and Nithya Heller and Arunkumar Dorai and Hema Muthusamy",

year = "2012",

doi = "10.1166/jnn.2012.5362",

language = "English",

volume = "12",

pages = "737--742",

journal = "Journal of Nanoscience and Nanotechnology",

issn = "1533-4880",

publisher = "American Scientific Publishers",

number = "1",

}

TY - JOUR

T1 - Synthesis of Li 1+x V 3O 8 by chemical route and its characterization

AU - Subramanian, Selvasekarapandian

AU - Ayyasamy, Sakunthala

AU - Selvin, P. Christopher

AU - Reddy, M. V.

AU - Chowdari, B. V.R.

AU - Heller, Nithya

AU - Dorai, Arunkumar

AU - Muthusamy, Hema

PY - 2012

Y1 - 2012

N2 - Lithium trivanadate (Li 1+xV 3O 8) nanorods have been synthesized by the simple polymer precursor route using the polymer, polyvinyl pyrrolidone (PVP) as the complexing agent. Thermal behavior of the precursor has been studied by the differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and differential thermal analysis (DTA) techniques. X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) studies confirm the formation of the compound. High resolution scanning electron microscopy (HRSEM) analysis reveals the synthesized Li 1.2V 3O 8 particles to be nanorods with an average diameter of 50 nm.

AB - Lithium trivanadate (Li 1+xV 3O 8) nanorods have been synthesized by the simple polymer precursor route using the polymer, polyvinyl pyrrolidone (PVP) as the complexing agent. Thermal behavior of the precursor has been studied by the differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and differential thermal analysis (DTA) techniques. X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) studies confirm the formation of the compound. High resolution scanning electron microscopy (HRSEM) analysis reveals the synthesized Li 1.2V 3O 8 particles to be nanorods with an average diameter of 50 nm.

KW - Cathode material

KW - Conductivity

KW - Li V O

KW - Nanorods

KW - PVP

UR - http://www.scopus.com/inward/record.url?scp=84861114074&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=84861114074&partnerID=8YFLogxK

U2 - 10.1166/jnn.2012.5362

DO - 10.1166/jnn.2012.5362

M3 - Article

C2 - 22524049

AN - SCOPUS:84861114074

SN - 1533-4880

VL - 12

SP - 737

EP - 742

JO - Journal of Nanoscience and Nanotechnology

JF - Journal of Nanoscience and Nanotechnology

IS - 1

ER -

Synthesis of Li _1+x V ₃O ₈ by chemical route and its characterization

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this