The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis

Klaus Peter Jochum; Donald B. Dingwell; Alexander Rocholl; Brigitte Stoll; Albrecht W. Hofmann; S. Becker; A. Besmehn; D. Besserte; H. J. Dietze; P. Dulski; J. Erzinger; E. Hellebrand; P. Hoppe; I. Horn; K. Janssens; G. A. Jenner; M. Klein; W. F. McDonough; M. Maetz; K. Mezger; C. Münker; I. K. Nikogosian; C. Pickhardt; I. Raczek; D. Rhede; H. M. Seufert; S. G. Simakin; A. V. Sobolev; B. Spettel; S. Straub; L. Vincze; A. Wallianos; G. Weckwerth; S. Weyer; D. Wolf; M. Zimmer

doi:10.1111/j.1751-908X.2000.tb00590.x

The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis

Klaus Peter Jochum, Donald B. Dingwell, Alexander Rocholl, Brigitte Stoll, Albrecht W. Hofmann, S. Becker, A. Besmehn, D. Besserte, H. J. Dietze, P. Dulski, J. Erzinger, E. Hellebrand, P. Hoppe, I. Horn, K. Janssens, G. A. Jenner, M. Klein, W. F. McDonough, M. Maetz, K. MezgerC. Münker, I. K. Nikogosian, C. Pickhardt, I. Raczek, D. Rhede, H. M. Seufert, S. G. Simakin, A. V. Sobolev, B. Spettel, S. Straub, L. Vincze, A. Wallianos, G. Weckwerth, S. Weyer, D. Wolf, M. Zimmer

Research output: Contribution to journal › Article › peer-review

270 Citations (Scopus)

Abstract

Eight silicate glasses were prepared by directly fusing and stirring 50-100 g each of basalt, andesite, komatiite, peridotite, rhyolite, and quartz-diorite. These are referred to as MPI-DING glasses and were made for the purpose of providing reference materials for geochemical, in-situ microanalytical work. Results from various analytical techniques indicate that individual glass fragments are well homogenised with respect to major and trace elements at the μm to mm scale. Heterogeneities due to quench crystallisation of olivine have been observed in small and limited areas of the two komatiitic glasses. In order to obtain concentration values for as many elements as possible, the glasses were analysed by a variety of bulk and microanalytical methods in a number of laboratories. From the analytical data, preliminary reference values for more than sixty elements were calculated. The analytical uncertainties of most elements are estimated to be between 1% and 10%.

Original language	English
Pages (from-to)	87-133
Number of pages	47
Journal	Geostandards Newsletter
Volume	24
Issue number	1
DOIs	https://doi.org/10.1111/j.1751-908X.2000.tb00590.x
Publication status	Published - 2000
Externally published	Yes

Keywords

Characterisation
Geological glasses
In-situ techniques
Microprobe analysis
Preparation
Reference materials

ASJC Scopus subject areas

Geology
Geochemistry and Petrology

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10.1111/j.1751-908X.2000.tb00590.x

Cite this

Jochum, K. P., Dingwell, D. B., Rocholl, A., Stoll, B., Hofmann, A. W., Becker, S., Besmehn, A., Besserte, D., Dietze, H. J., Dulski, P., Erzinger, J., Hellebrand, E., Hoppe, P., Horn, I., Janssens, K., Jenner, G. A., Klein, M., McDonough, W. F., Maetz, M., ... Zimmer, M. (2000). The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis. Geostandards Newsletter, 24(1), 87-133. https://doi.org/10.1111/j.1751-908X.2000.tb00590.x

Jochum, KP, Dingwell, DB, Rocholl, A, Stoll, B, Hofmann, AW, Becker, S, Besmehn, A, Besserte, D, Dietze, HJ, Dulski, P, Erzinger, J, Hellebrand, E, Hoppe, P, Horn, I, Janssens, K, Jenner, GA, Klein, M, McDonough, WF, Maetz, M, Mezger, K, Münker, C, Nikogosian, IK, Pickhardt, C, Raczek, I, Rhede, D, Seufert, HM, Simakin, SG, Sobolev, AV, Spettel, B, Straub, S, Vincze, L, Wallianos, A, Weckwerth, G, Weyer, S, Wolf, D & Zimmer, M 2000, 'The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis', Geostandards Newsletter, vol. 24, no. 1, pp. 87-133. https://doi.org/10.1111/j.1751-908X.2000.tb00590.x

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title = "The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis",

abstract = "Eight silicate glasses were prepared by directly fusing and stirring 50-100 g each of basalt, andesite, komatiite, peridotite, rhyolite, and quartz-diorite. These are referred to as MPI-DING glasses and were made for the purpose of providing reference materials for geochemical, in-situ microanalytical work. Results from various analytical techniques indicate that individual glass fragments are well homogenised with respect to major and trace elements at the μm to mm scale. Heterogeneities due to quench crystallisation of olivine have been observed in small and limited areas of the two komatiitic glasses. In order to obtain concentration values for as many elements as possible, the glasses were analysed by a variety of bulk and microanalytical methods in a number of laboratories. From the analytical data, preliminary reference values for more than sixty elements were calculated. The analytical uncertainties of most elements are estimated to be between 1% and 10%.",

keywords = "Characterisation, Geological glasses, In-situ techniques, Microprobe analysis, Preparation, Reference materials",

author = "Jochum, {Klaus Peter} and Dingwell, {Donald B.} and Alexander Rocholl and Brigitte Stoll and Hofmann, {Albrecht W.} and S. Becker and A. Besmehn and D. Besserte and Dietze, {H. J.} and P. Dulski and J. Erzinger and E. Hellebrand and P. Hoppe and I. Horn and K. Janssens and Jenner, {G. A.} and M. Klein and McDonough, {W. F.} and M. Maetz and K. Mezger and C. M{\"u}nker and Nikogosian, {I. K.} and C. Pickhardt and I. Raczek and D. Rhede and Seufert, {H. M.} and Simakin, {S. G.} and Sobolev, {A. V.} and B. Spettel and S. Straub and L. Vincze and A. Wallianos and G. Weckwerth and S. Weyer and D. Wolf and M. Zimmer",

year = "2000",

doi = "10.1111/j.1751-908X.2000.tb00590.x",

language = "English",

volume = "24",

pages = "87--133",

journal = "Geostandards and Geoanalytical Research",

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T1 - The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis

AU - Jochum, Klaus Peter

AU - Dingwell, Donald B.

AU - Rocholl, Alexander

AU - Stoll, Brigitte

AU - Hofmann, Albrecht W.

AU - Becker, S.

AU - Besmehn, A.

AU - Besserte, D.

AU - Dietze, H. J.

AU - Dulski, P.

AU - Erzinger, J.

AU - Hellebrand, E.

AU - Hoppe, P.

AU - Horn, I.

AU - Janssens, K.

AU - Jenner, G. A.

AU - Klein, M.

AU - McDonough, W. F.

AU - Maetz, M.

AU - Mezger, K.

AU - Münker, C.

AU - Nikogosian, I. K.

AU - Pickhardt, C.

AU - Raczek, I.

AU - Rhede, D.

AU - Seufert, H. M.

AU - Simakin, S. G.

AU - Sobolev, A. V.

AU - Spettel, B.

AU - Straub, S.

AU - Vincze, L.

AU - Wallianos, A.

AU - Weckwerth, G.

AU - Weyer, S.

AU - Wolf, D.

AU - Zimmer, M.

PY - 2000

Y1 - 2000

N2 - Eight silicate glasses were prepared by directly fusing and stirring 50-100 g each of basalt, andesite, komatiite, peridotite, rhyolite, and quartz-diorite. These are referred to as MPI-DING glasses and were made for the purpose of providing reference materials for geochemical, in-situ microanalytical work. Results from various analytical techniques indicate that individual glass fragments are well homogenised with respect to major and trace elements at the μm to mm scale. Heterogeneities due to quench crystallisation of olivine have been observed in small and limited areas of the two komatiitic glasses. In order to obtain concentration values for as many elements as possible, the glasses were analysed by a variety of bulk and microanalytical methods in a number of laboratories. From the analytical data, preliminary reference values for more than sixty elements were calculated. The analytical uncertainties of most elements are estimated to be between 1% and 10%.

AB - Eight silicate glasses were prepared by directly fusing and stirring 50-100 g each of basalt, andesite, komatiite, peridotite, rhyolite, and quartz-diorite. These are referred to as MPI-DING glasses and were made for the purpose of providing reference materials for geochemical, in-situ microanalytical work. Results from various analytical techniques indicate that individual glass fragments are well homogenised with respect to major and trace elements at the μm to mm scale. Heterogeneities due to quench crystallisation of olivine have been observed in small and limited areas of the two komatiitic glasses. In order to obtain concentration values for as many elements as possible, the glasses were analysed by a variety of bulk and microanalytical methods in a number of laboratories. From the analytical data, preliminary reference values for more than sixty elements were calculated. The analytical uncertainties of most elements are estimated to be between 1% and 10%.

KW - Characterisation

KW - Geological glasses

KW - In-situ techniques

KW - Microprobe analysis

KW - Preparation

KW - Reference materials

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DO - 10.1111/j.1751-908X.2000.tb00590.x

M3 - Article

AN - SCOPUS:33745158272

SN - 1639-4488

VL - 24

SP - 87

EP - 133

JO - Geostandards and Geoanalytical Research

JF - Geostandards and Geoanalytical Research

IS - 1

ER -

The preparation and preliminary characterisation of eight geological MPI-DING reference glasses for in-situ microanalysis

Abstract

Keywords

ASJC Scopus subject areas

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